Browsing by Author "Briggs, Lisa"
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Item Open Access 6 Shipwreck archaeology in the past 10 years(Cambridge University Press (CUP), 2023-12-08) Briggs, Lisa; Campbell, Peter B.This paper reviews the trends, topics, and research directions in shipwreck archaeology over the past decade. As archaeology increasingly embraces advances in technological methods that can aid our research, the so-called ‘digital turn’, it behoves maritime archaeologists, and archaeologists more broadly, to consider how collaborative utilization of specialized fields including biomolecular archaeology, geophysics, and contemporary philosophy have spurred on a rapid modernization of our field in recent times. Archaeological research, both terrestrial and underwater, has long been a collaborative discipline. However, we argue here that difficulties in working underwater have encouraged maritime and underwater archaeologists to embrace technological developments at a rapid pace. An explicit theoretical framework and the incorporation of contemporary philosophy in the field of underwater archaeology was, until recently, largely lacking in the discipline’s discourse. The incorporation and advancement of adjacent disciplines within the field of underwater archaeology mark the most relevant changes within the shifting tides of shipwreck research.Item Open Access Advances in the characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples by GC-QToF-MS(Royal Society of Chemistry (RSC), 2024-01-02) Tamburini, Diego; Fulcher, Kate; Briggs, Lisa; von Aderkas, Nelly; Pulak, Cemal; Stacey, RebeccaThe optimisation and application of an analytical method based on gas chromatography coupled to quadrupole time-of-flight mass spectrometry (GC-QToF-MS) is proposed for the first time for the characterisation and identification of mastic (Pistacia sp.) resin in archaeological samples. The GC-QToF-MS method demonstrated higher sensitivity compared to single quadrupole GC-MS and enabled enhanced structural elucidation power to be exploited, particularly due to the high mass resolution and accuracy, the possibility to use standard and low ionisation energies as well as its tandem MS capabilities. The heat-induced degradation of the resin was also studied in open air conditions, showing that 28-norolean-17-en-3-one forms upon heating, but then progressively degrades. This makes it a reliable marker for heating of Pistacia resin; however, the lack of detection does not imply that the resin was not heated. These observations were used to interpret the results of a large number of archaeological samples containing Pistacia resin in different formulations, from various archaeological contexts and exposed to different environmental conditions. Lumps of relatively pure resin found in marine waterlogged conditions (Uluburun shipwreck, Turkey), residues on ceramics from Sai Island (Nubia, Sudan) as well as varnish and coating layers on Egyptian coffins from the collections of the British Museum (London, UK) and Fitzwilliam Museum (Cambridge, UK) were analysed to understand what the molecular profiles reveal about the use of the resin. The results showed that the resin was often mixed with a drying or semi-drying oil in ancient varnish formulations, thus suggesting that oil was used as a medium to dissolve the resin, which would have been impossible to apply as a layer using simple heat. These new observations significantly add to our understanding of ancient Egyptian technology and provide museum scientists and conservators with key information to accurately identify Pistacia resin and preserve objects containing it.Item Open Access Molecular evidence for new foodways in the early colonial Caribbean: organic residue analysis at Isla de Mona, Puerto Rico(Springer, 2023-05-03) Briggs, Lisa; Cooper, Jago; Craig, Oliver E.; Heron, Carl; Lucquin, Alexandre; Milantchi, María Mercedes Martínez; Samson, AliceCeramic objects account for over 90% of the cultural material recovered from archaeological sites in the Caribbean. However, little research has been conducted on molecular evidence for past food production from these same vessels. Forty ceramic sherds from Isla de Mona have been analysed by GC–MS and GC-C-IRMS in order to address questions surrounding foodways in the Greater Antilles prior to and post European arrival. We evaluate evidence for dietary changes to illuminate aspects of cultural exchange between Indigenous populations and the first generations of Spanish colonists. Here, we show that plant residues are found in a variety of pottery forms, with some evidence for non-ruminant and ruminant fats. The dearth of marine biomarkers is curious given the volume of fish bones found in archaeological contexts on Isla de Mona and may offer evidence for spit-roasting, pit-roasting, or the use of a ‘barbacoa’ to cook fish on the island. The ubiquity of plant residues in a variety of pottery forms may relate to the large-scale cultivation and export of cassava (Manihot esculenta) from the island. A Spanish olive jar revealed evidence of wine residues, which may constitute the earliest detection of wine residues in pottery found in the Americas.